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Synthesis of ROS-sensitive polymers conjugated with Ru(II)-OH (P4) At room temperature, 4-Dimethylaminopyridine (DMAP, 126 mg) was introduced to a solution of Ru(II)-OH (50 mg) and 1-(3-Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDCl, 200 mg)

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The model demonstrated that exposure ratios between the subgroups were similar or slightly smaller on day 10 compared with steady state (details not shown), thereby confirming that the primary conclusions regarding exposure ratios across the 10-day trials are applicable at steady state